Determination of Young’s Modulus in Triglycine Sulfate Crystals with Layered Impurity Distribution
Abstract A technique for studying the local elastic properties of inhomogeneous ferroelectrics has been proposed by the example of growth striations in triglycine sulfate crystals, layer-by-layer doped with chromium and L-α-alanine impurities. The data on the width and impurity compositions of stripes were obtained by X-ray fluorescence analysis and X-ray topography. The positions of the boundaries of the stripes emerging at the surface and the domain structure morphology were determined by the methods of correlation electrical atomic-force microscopy. The force curves were measured and Young’s moduli were calculated for impurity-free and doped crystal stripes using contact atomic-force spectroscopy. The introduction of impurity decreases Young’s modulus: the difference was found to be 20–25 and 12–14% for chromium and L-α-alanine, respectively..
Medienart: |
E-Artikel |
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Erscheinungsjahr: |
2022 |
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Erschienen: |
2022 |
Enthalten in: |
Zur Gesamtaufnahme - volume:67 |
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Enthalten in: |
Crystallography reports - 67(2022), 4 vom: 22. Juli, Seite 594-601 |
Sprache: |
Englisch |
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Beteiligte Personen: |
Gainutdinov, R. V. [VerfasserIn] |
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Links: |
Volltext [lizenzpflichtig] |
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Anmerkungen: |
© Pleiades Publishing, Inc. 2022. ISSN 1063-7745, Crystallography Reports, 2022, Vol. 67, No. 4, pp. 594–601. © Pleiades Publishing, Inc., 2022. Russian Text © The Author(s), 2022, published in Kristallografiya, 2022, Vol. 67, No. 4, pp. 636–644. |
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doi: |
10.1134/S1063774522040095 |
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funding: |
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Förderinstitution / Projekttitel: |
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PPN (Katalog-ID): |
OLC2131413289 |
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520 | |a Abstract A technique for studying the local elastic properties of inhomogeneous ferroelectrics has been proposed by the example of growth striations in triglycine sulfate crystals, layer-by-layer doped with chromium and L-α-alanine impurities. The data on the width and impurity compositions of stripes were obtained by X-ray fluorescence analysis and X-ray topography. The positions of the boundaries of the stripes emerging at the surface and the domain structure morphology were determined by the methods of correlation electrical atomic-force microscopy. The force curves were measured and Young’s moduli were calculated for impurity-free and doped crystal stripes using contact atomic-force spectroscopy. The introduction of impurity decreases Young’s modulus: the difference was found to be 20–25 and 12–14% for chromium and L-α-alanine, respectively. | ||
700 | 1 | |a Lashkova, A. K. |4 aut | |
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700 | 1 | |a Asadchikov, V. E. |4 aut | |
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700 | 1 | |a Roshchin, B. S. |4 aut | |
700 | 1 | |a Shut, V. N. |4 aut | |
700 | 1 | |a Kashevich, I. F. |4 aut | |
700 | 1 | |a Mozzharov, S. E. |4 aut | |
700 | 1 | |a Tolstikhina, A. L. |4 aut | |
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