Details der Publikation - The Synthesis and Crystal Structure of 5-Methyl-1-(1-naphthyl)-1,2,3-triazol-4-carboxyl Acid

The Synthesis and Crystal Structure of 5-Methyl-1-(1-naphthyl)-1,2,3-triazol-4-carboxyl Acid

Abstract 5-Methyl-1-(1-naphthyl)-1,2,3-triazol-4-carboxyl acid 3 was synthesized from 1-aminonaphthalene. The yielded product 3 was investigated with X-ray crystallographic, NMR, MS and IR techniques. Compound 3, $ C_{14} $$ H_{11} $$ N_{3} $$ O_{2} $, Mr = 253.26, crystallizes in the orthorhombic space group Pbca with unit cell parameters a = 10.068(2), b = 12.353(2), c = 20.102(4) Å, V = 2500.1(8) $ Å^{3} $, Z = 8, Dx = 1.346 $ Mgm^{-3} $. The final R was 0.0474. The molecular packing is stabilized by intermolecular O–H···N interactions. Index Abstract 5-Methyl-1-(1-naphthyl)-1,2,3-triazol-4-carboxyl acid 3 was synthesized from 1-aminonaphthalene. The yielded product 3 was investigated with X-ray crystallographic, NMR, MS and IR techniques. Compound 3, $ C_{14} $$ H_{11} $$ N_{3} $$ O_{2} $, Mr = 253.26, crystallizes in the orthorhombic space group Pbca with unit cell parameters a = 10.068(2), b = 12.353(2), c = 20.102(4) Å, α = β = γ = 90.00º. V = 2,500.1(8) $ Å^{3} $, Z = 8, Dx = 1.346 $ Mgm^{−3} $. The final R was 0.0474. The molecular packing is stabilized by intermolecular O–H···N interactions..

Medienart:	E-Artikel

Erscheinungsjahr:	2008
Erschienen:	2008

Enthalten in:	Zur Gesamtaufnahme - volume:39
Enthalten in:	Journal of chemical crystallography - 39(2008), 2 vom: 26. Juni, Seite 87-90

Sprache:	Englisch

Beteiligte Personen:	Liu, Shi-Qiang [VerfasserIn] Quan, Bin [VerfasserIn] Dong, Hong-Ru [VerfasserIn] Dong, Heng-Shan [VerfasserIn]

Links:	Volltext [lizenzpflichtig]

BKL:	35.25$jSpektrochemische Analyse 35.90$jFestkörperchemie 38.31$jKristallographie 51.00$jWerkstoffkunde: Allgemeines
Themen:	1,2,3-Triazol-4-carboxyl acid 5-Methyl-1-(1-naphthyl)-1,2,3-triazol-4-carboxyl acid Crystal structure H-bond Synthesis

Anmerkungen:	© Springer Science+Business Media, LLC 2008

doi:	10.1007/s10870-008-9408-9

funding:
Förderinstitution / Projekttitel:

PPN (Katalog-ID):	OLC2115397894

Internformat


LEADER	01000naa a22002652 4500
001	OLC2115397894
003	DE-627
005	20230503134047.0
007	cr uuu---uuuuu
008	230503s2008 xx \|\|\|\|\|o 00\| \|\|eng c
024	7		\|a 10.1007/s10870-008-9408-9 \|2 doi
035			\|a (DE-627)OLC2115397894
035			\|a (DE-He213)s10870-008-9408-9-e
040			\|a DE-627 \|b ger \|c DE-627 \|e rakwb
041			\|a eng
082	0	4	\|a 540 \|q VZ
084			\|a 35.25$jSpektrochemische Analyse \|2 bkl
084			\|a 35.90$jFestkörperchemie \|2 bkl
084			\|a 38.31$jKristallographie \|2 bkl
084			\|a 51.00$jWerkstoffkunde: Allgemeines \|2 bkl
100	1		\|a Liu, Shi-Qiang \|e verfasserin \|4 aut
245	1	0	\|a The Synthesis and Crystal Structure of 5-Methyl-1-(1-naphthyl)-1,2,3-triazol-4-carboxyl Acid
264		1	\|c 2008
336			\|a Text \|b txt \|2 rdacontent
337			\|a Computermedien \|b c \|2 rdamedia
338			\|a Online-Ressource \|b cr \|2 rdacarrier
500			\|a © Springer Science+Business Media, LLC 2008
520			\|a Abstract 5-Methyl-1-(1-naphthyl)-1,2,3-triazol-4-carboxyl acid 3 was synthesized from 1-aminonaphthalene. The yielded product 3 was investigated with X-ray crystallographic, NMR, MS and IR techniques. Compound 3, $ C_{14} $$ H_{11} $$ N_{3} $$ O_{2} $, Mr = 253.26, crystallizes in the orthorhombic space group Pbca with unit cell parameters a = 10.068(2), b = 12.353(2), c = 20.102(4) Å, V = 2500.1(8) $ Å^{3} $, Z = 8, Dx = 1.346 $ Mgm^{-3} $. The final R was 0.0474. The molecular packing is stabilized by intermolecular O–H···N interactions. Index Abstract 5-Methyl-1-(1-naphthyl)-1,2,3-triazol-4-carboxyl acid 3 was synthesized from 1-aminonaphthalene. The yielded product 3 was investigated with X-ray crystallographic, NMR, MS and IR techniques. Compound 3, $ C_{14} $$ H_{11} $$ N_{3} $$ O_{2} $, Mr = 253.26, crystallizes in the orthorhombic space group Pbca with unit cell parameters a = 10.068(2), b = 12.353(2), c = 20.102(4) Å, α = β = γ = 90.00º. V = 2,500.1(8) $ Å^{3} $, Z = 8, Dx = 1.346 $ Mgm^{−3} $. The final R was 0.0474. The molecular packing is stabilized by intermolecular O–H···N interactions.
650		4	\|a Crystal structure
650		4	\|a 1,2,3-Triazol-4-carboxyl acid
650		4	\|a 5-Methyl-1-(1-naphthyl)-1,2,3-triazol-4-carboxyl acid
650		4	\|a H-bond
650		4	\|a Synthesis
700	1		\|a Quan, Bin \|4 aut
700	1		\|a Dong, Hong-Ru \|4 aut
700	1		\|a Dong, Heng-Shan \|4 aut
773	0	8	\|i Enthalten in \|t Journal of chemical crystallography \|d Springer US, 1971 \|g 39(2008), 2 vom: 26. Juni, Seite 87-90 \|h Online-Ressource \|w (DE-627)302467270 \|w (DE-600)1491232-6 \|w (DE-576)104082208 \|x 1572-8854 \|7 nnns
773	1	8	\|g volume:39 \|g year:2008 \|g number:2 \|g day:26 \|g month:06 \|g pages:87-90
856	4	0	\|u https://dx.doi.org/10.1007/s10870-008-9408-9 \|z lizenzpflichtig \|3 Volltext
912			\|a GBV_USEFLAG_A
912			\|a SYSFLAG_A
912			\|a GBV_OLC
912			\|a SSG-OPC-GGO
912			\|a GBV_ILN_11
912			\|a GBV_ILN_20
912			\|a GBV_ILN_22
912			\|a GBV_ILN_23
912			\|a GBV_ILN_31
912			\|a GBV_ILN_32
912			\|a GBV_ILN_39
912			\|a GBV_ILN_40
912			\|a GBV_ILN_60
912			\|a GBV_ILN_62
912			\|a GBV_ILN_63
912			\|a GBV_ILN_69
912			\|a GBV_ILN_70
912			\|a GBV_ILN_73
912			\|a GBV_ILN_74
912			\|a GBV_ILN_90
912			\|a GBV_ILN_95
912			\|a GBV_ILN_100
912			\|a GBV_ILN_101
912			\|a GBV_ILN_105
912			\|a GBV_ILN_110
912			\|a GBV_ILN_120
912			\|a GBV_ILN_138
912			\|a GBV_ILN_150
912			\|a GBV_ILN_151
912			\|a GBV_ILN_152
912			\|a GBV_ILN_161
912			\|a GBV_ILN_170
912			\|a GBV_ILN_187
912			\|a GBV_ILN_213
912			\|a GBV_ILN_230
912			\|a GBV_ILN_285
912			\|a GBV_ILN_293
912			\|a GBV_ILN_370
912			\|a GBV_ILN_602
912			\|a GBV_ILN_636
912			\|a GBV_ILN_702
912			\|a GBV_ILN_2001
912			\|a GBV_ILN_2003
912			\|a GBV_ILN_2004
912			\|a GBV_ILN_2005
912			\|a GBV_ILN_2006
912			\|a GBV_ILN_2007
912			\|a GBV_ILN_2008
912			\|a GBV_ILN_2009
912			\|a GBV_ILN_2010
912			\|a GBV_ILN_2011
912			\|a GBV_ILN_2014
912			\|a GBV_ILN_2015
912			\|a GBV_ILN_2020
912			\|a GBV_ILN_2021
912			\|a GBV_ILN_2025
912			\|a GBV_ILN_2026
912			\|a GBV_ILN_2027
912			\|a GBV_ILN_2031
912			\|a GBV_ILN_2034
912			\|a GBV_ILN_2037
912			\|a GBV_ILN_2038
912			\|a GBV_ILN_2039
912			\|a GBV_ILN_2044
912			\|a GBV_ILN_2048
912			\|a GBV_ILN_2049
912			\|a GBV_ILN_2055
912			\|a GBV_ILN_2057
912			\|a GBV_ILN_2059
912			\|a GBV_ILN_2061
912			\|a GBV_ILN_2064
912			\|a GBV_ILN_2065
912			\|a GBV_ILN_2068
912			\|a GBV_ILN_2070
912			\|a GBV_ILN_2086
912			\|a GBV_ILN_2088
912			\|a GBV_ILN_2093
912			\|a GBV_ILN_2106
912			\|a GBV_ILN_2107
912			\|a GBV_ILN_2108
912			\|a GBV_ILN_2110
912			\|a GBV_ILN_2111
912			\|a GBV_ILN_2112
912			\|a GBV_ILN_2113
912			\|a GBV_ILN_2116
912			\|a GBV_ILN_2118
912			\|a GBV_ILN_2119
912			\|a GBV_ILN_2122
912			\|a GBV_ILN_2129
912			\|a GBV_ILN_2132
912			\|a GBV_ILN_2134
912			\|a GBV_ILN_2143
912			\|a GBV_ILN_2144
912			\|a GBV_ILN_2147
912			\|a GBV_ILN_2148
912			\|a GBV_ILN_2152
912			\|a GBV_ILN_2153
912			\|a GBV_ILN_2188
912			\|a GBV_ILN_2190
912			\|a GBV_ILN_2232
912			\|a GBV_ILN_2336
912			\|a GBV_ILN_2433
912			\|a GBV_ILN_2446
912			\|a GBV_ILN_2470
912			\|a GBV_ILN_2474
912			\|a GBV_ILN_2507
912			\|a GBV_ILN_2522
912			\|a GBV_ILN_2548
912			\|a GBV_ILN_4012
912			\|a GBV_ILN_4035
912			\|a GBV_ILN_4037
912			\|a GBV_ILN_4046
912			\|a GBV_ILN_4112
912			\|a GBV_ILN_4125
912			\|a GBV_ILN_4126
912			\|a GBV_ILN_4242
912			\|a GBV_ILN_4246
912			\|a GBV_ILN_4249
912			\|a GBV_ILN_4251
912			\|a GBV_ILN_4305
912			\|a GBV_ILN_4306
912			\|a GBV_ILN_4307
912			\|a GBV_ILN_4313
912			\|a GBV_ILN_4322
912			\|a GBV_ILN_4323
912			\|a GBV_ILN_4324
912			\|a GBV_ILN_4325
912			\|a GBV_ILN_4326
912			\|a GBV_ILN_4333
912			\|a GBV_ILN_4334
912			\|a GBV_ILN_4335
912			\|a GBV_ILN_4336
912			\|a GBV_ILN_4338
912			\|a GBV_ILN_4393
912			\|a GBV_ILN_4700
936	b	k	\|a 35.25$jSpektrochemische Analyse \|q VZ \|0 106419218 \|0 (DE-625)106419218
936	b	k	\|a 35.90$jFestkörperchemie \|q VZ \|0 106419293 \|0 (DE-625)106419293
936	b	k	\|a 38.31$jKristallographie \|q VZ \|0 181570114 \|0 (DE-625)181570114
936	b	k	\|a 51.00$jWerkstoffkunde: Allgemeines \|q VZ \|0 106410989 \|0 (DE-625)106410989
951			\|a AR
952			\|d 39 \|j 2008 \|e 2 \|b 26 \|c 06 \|h 87-90

The Synthesis and Crystal Structure of 5-Methyl-1-(1-naphthyl)-1,2,3-triazol-4-carboxyl Acid

Zugang & Verfügbarkeit

Zugehörige Publikationen/Bände