Development of porous and dispersed CRM

Abstract Porous and finely dispersed certified reference materials (CRM) were certified using the gas adsorption method. The special certification procedure for IUPAC isotherm classification types I, II, and IV is presented for meso- and macroporous materials with special emphasis on specific surface area, specific pore volume and pore width according to standards DIN 66 131, 66 134, and 66 135. Four CRMs ($ SiO_{2} $, α-$ Al_{2} $$ O_{3} $, two transition aluminas) with a macro- and mesopore range are presented. Certification was made on the basis of BCR guidelines in connection with interlaboratory tests (altogether 38 participating laboratories, 44 various gas adsorption apparatus)..

Medienart:

Artikel

Erscheinungsjahr:

1998

Erschienen:

1998

Enthalten in:

Zur Gesamtaufnahme - volume:360

Enthalten in:

Fresenius' journal of analytical chemistry - 360(1998), 3-4 vom: 01. Feb., Seite 393-397

Sprache:

Englisch

Beteiligte Personen:

Röhl-Kuhn, B. [VerfasserIn]
Meyer, K. [VerfasserIn]
Klobes, P. [VerfasserIn]
Fritz, T. [VerfasserIn]

Links:

Volltext [lizenzpflichtig]

Themen:

Certify Reference Material
Classification Type
Meso
Pore Volume
SiO2

Anmerkungen:

© Springer-Verlag Berlin Heidelberg 1998

doi:

10.1007/s002160050720

funding:

Förderinstitution / Projekttitel:

PPN (Katalog-ID):

OLC2090062975