Concise synthesis of the C15-C38 fragment of okadaic acid: application of the Suzuki-Miyaura reaction to spiroacetal synthesis
A concise synthetic entry to the C15-C38 fragment of okadaic acid by exploiting a Suzuki-Miyaura reaction for the rapid assembly of the spiroacetal substructures has been developed. The present synthesis was completed in 19 linear steps from a commercially available material, showcasing the efficiency of our synthetic strategy..
| Medienart: |
Artikel |
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| Erscheinungsjahr: |
2015 |
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| Erschienen: |
2015 |
| Enthalten in: |
Zur Gesamtaufnahme - volume:17 |
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| Enthalten in: |
Organic letters - 17(2015), 2, Seite 366 |
| Sprache: |
Englisch |
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| Beteiligte Personen: |
Fuwa, Haruhiko [VerfasserIn] |
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OLC1960813862 |
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| 245 | 1 | 0 | |a Concise synthesis of the C15-C38 fragment of okadaic acid: application of the Suzuki-Miyaura reaction to spiroacetal synthesis |
| 264 | 1 | |c 2015 | |
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| 520 | |a A concise synthetic entry to the C15-C38 fragment of okadaic acid by exploiting a Suzuki-Miyaura reaction for the rapid assembly of the spiroacetal substructures has been developed. The present synthesis was completed in 19 linear steps from a commercially available material, showcasing the efficiency of our synthetic strategy. | ||
| 650 | 4 | |a Carbon Isotopes - chemistry | |
| 650 | 4 | |a Spiro Compounds - chemistry | |
| 650 | 4 | |a Okadaic Acid - chemical synthesis | |
| 650 | 4 | |a Okadaic Acid - chemistry | |
| 650 | 4 | |a Spiro Compounds - chemical synthesis | |
| 650 | 4 | |a Acetals - chemical synthesis | |
| 650 | 4 | |a Acetals - chemistry | |
| 700 | 1 | |a Sakamoto, Keita |4 oth | |
| 700 | 1 | |a Muto, Takashi |4 oth | |
| 700 | 1 | |a Sasaki, Makoto |4 oth | |
| 773 | 0 | 8 | |i Enthalten in |t Organic letters |d Washington, DC [u.a.] : Soc., 1999 |g 17(2015), 2, Seite 366 |w (DE-627)253386241 |w (DE-600)1458039-1 |w (DE-576)078991811 |x 1523-7060 |7 nnns |
| 773 | 1 | 8 | |g volume:17 |g year:2015 |g number:2 |g pages:366 |
| 856 | 4 | 2 | |u http://www.ncbi.nlm.nih.gov/pubmed/25544331 |
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