High enrichment and sensitive measurement of oxytetracycline in tea drinks by thermosensitive magnetic molecular imprinting based magnetic solid phase extraction coupled with boron doped carbon dots

Copyright © 2023. Published by Elsevier Ltd..

As a typical kind of new pollutants, there are still some challenges in the rapid detection of antibiotics. In this work, a sensitive fluorescent probe based on boron-doped carbon dots (B-CDs) in combination with thermo-responsive magnetic molecularly imprinted polymers (T-MMIPs) was constructed for the detection of oxytetracycline (OTC) in tea drinks. T-MMIPs were designed, fabricated and employed to enrich OTC at trace level from tea drinks, and B-CDs were utilized as the fluorescent probe to detect the concentration of OTC. The proposed method exhibited good linear relationship with OTC concentration from 0.2 to 60 μg L-1 and the limit of detection was 0.1 μg L-1. The established method has been successfully validated with tea beverages. Present work was the first attempt application of T-MMIPs in combination with CDs in detection of OTC, and demonstrated that the proposed method endowed the detection of OTC with high selectivity, sensitivity, reliability and wide application prospect, meanwhile offered a new strategy for the method establishment of rapid and sensitive detection of trace antibiotics in food and other matrices.

Medienart:

E-Artikel

Erscheinungsjahr:

2024

Erschienen:

2024

Enthalten in:

Zur Gesamtaufnahme - volume:447

Enthalten in:

Food chemistry - 447(2024) vom: 30. Apr., Seite 138998

Sprache:

Englisch

Beteiligte Personen:

Li, Zhi [VerfasserIn]
Li, Shuangying [VerfasserIn]
Jiang, Liushan [VerfasserIn]
Niu, Jingwen [VerfasserIn]
Zhang, Yue [VerfasserIn]
Nie, Linchun [VerfasserIn]
Zhou, Qingxiang [VerfasserIn]
Chen, Chunmao [VerfasserIn]

Links:

Volltext

Themen:

7440-44-0
Anti-Bacterial Agents
Boron
Boron doped carbon dots
Carbon
Fluorescence spectrometry
Fluorescent Dyes
Journal Article
Magnetic solid phase extraction
N9E3X5056Q
Oxytetracycline
Polymers
Tea
Thermosensitive magnetic molecularly imprinted polymers
X20I9EN955

Anmerkungen:

Date Completed 10.04.2024

Date Revised 10.04.2024

published: Print-Electronic

Citation Status MEDLINE

doi:

10.1016/j.foodchem.2024.138998

funding:

Förderinstitution / Projekttitel:

PPN (Katalog-ID):

NLM369926757