Iodine-catalyzed regioselective direct sulfenylation of uracil with sulfonyl hydrazide as sulfur source under solvent free conditions
This journal is © The Royal Society of Chemistry..
A facile method was developed for the selective thioetherification of uracils using sulfonyl hydrazide as the thioetherification reagent. This method offers advantages such as avoiding the use of additives and expensive metal catalysts, and providing good to excellent yields of various uracil thioethers. Experimental studies have demonstrated that the reaction follows a free radical pathway. Notably, the reaction can be carried out without solvent.
| Medienart: |
E-Artikel |
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| Erscheinungsjahr: |
2024 |
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| Erschienen: |
2024 |
| Enthalten in: |
Zur Gesamtaufnahme - volume:14 |
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| Enthalten in: |
RSC advances - 14(2024), 7 vom: 31. Jan., Seite 4587-4590 |
| Sprache: |
Englisch |
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| Beteiligte Personen: |
Wang, Cong [VerfasserIn] |
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| Links: |
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| Themen: |
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| Anmerkungen: |
Date Revised 07.02.2024 published: Electronic-eCollection Citation Status PubMed-not-MEDLINE |
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| doi: |
10.1039/d3ra07398j |
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| funding: |
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| Förderinstitution / Projekttitel: |
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| 520 | |a This journal is © The Royal Society of Chemistry. | ||
| 520 | |a A facile method was developed for the selective thioetherification of uracils using sulfonyl hydrazide as the thioetherification reagent. This method offers advantages such as avoiding the use of additives and expensive metal catalysts, and providing good to excellent yields of various uracil thioethers. Experimental studies have demonstrated that the reaction follows a free radical pathway. Notably, the reaction can be carried out without solvent | ||
| 650 | 4 | |a Journal Article | |
| 700 | 1 | |a Peng, Qi-Yun |e verfasserin |4 aut | |
| 700 | 1 | |a Wu, Yi |e verfasserin |4 aut | |
| 700 | 1 | |a He, Yan-Ling |e verfasserin |4 aut | |
| 700 | 1 | |a Zheng, Xiao-He |e verfasserin |4 aut | |
| 700 | 1 | |a Wang, Hai-Bo |e verfasserin |4 aut | |
| 700 | 1 | |a Xin, Jia-Min |e verfasserin |4 aut | |
| 700 | 1 | |a He, Qing |e verfasserin |4 aut | |
| 700 | 1 | |a Xie, Jun |e verfasserin |4 aut | |
| 700 | 1 | |a Tang, Lei |e verfasserin |4 aut | |
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