The lower energy diffraction and scattering side-bounce beamline for materials science at the Canadian Light Source
A new diffraction beamline for materials science has been built at the Canadian Light Source synchrotron. The X-ray source is an in-vacuum wiggler with a 2.5 T peak magnetic field at 5.2 mm gap. The optical configuration includes a toroidal mirror, a single side-bounce Bragg monochromator, and a cylindrical mirror, producing a sub-150 µm vertical × 500 µm horizontal focused beam with a photon energy range of 7-22 keV and a flux of 1012 photons per second at the sample position. Three endstations are currently open to general users, and the techniques available include high-resolution powder diffraction, small molecule crystallography, X-ray reflectivity, in situ rapid thermal annealing, and SAXS/WAXS. The beamline design parameters, calculated and measured performance, and initial experimental results are presented to demonstrate the capabilities for materials science.
Medienart: |
E-Artikel |
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Erscheinungsjahr: |
2021 |
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Erschienen: |
2021 |
Enthalten in: |
Zur Gesamtaufnahme - volume:28 |
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Enthalten in: |
Journal of synchrotron radiation - 28(2021), Pt 3 vom: 01. Mai, Seite 961-969 |
Sprache: |
Englisch |
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Beteiligte Personen: |
Leontowich, Adam F G [VerfasserIn] |
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Links: |
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Themen: |
Hard X-ray diffraction |
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Anmerkungen: |
Date Revised 06.05.2021 published: Print-Electronic Citation Status PubMed-not-MEDLINE |
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doi: |
10.1107/S1600577521002496 |
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funding: |
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Förderinstitution / Projekttitel: |
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PPN (Katalog-ID): |
NLM325028958 |
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520 | |a A new diffraction beamline for materials science has been built at the Canadian Light Source synchrotron. The X-ray source is an in-vacuum wiggler with a 2.5 T peak magnetic field at 5.2 mm gap. The optical configuration includes a toroidal mirror, a single side-bounce Bragg monochromator, and a cylindrical mirror, producing a sub-150 µm vertical × 500 µm horizontal focused beam with a photon energy range of 7-22 keV and a flux of 1012 photons per second at the sample position. Three endstations are currently open to general users, and the techniques available include high-resolution powder diffraction, small molecule crystallography, X-ray reflectivity, in situ rapid thermal annealing, and SAXS/WAXS. The beamline design parameters, calculated and measured performance, and initial experimental results are presented to demonstrate the capabilities for materials science | ||
650 | 4 | |a Journal Article | |
650 | 4 | |a X-ray scattering | |
650 | 4 | |a hard X-ray diffraction | |
650 | 4 | |a in-vacuum wiggler | |
650 | 4 | |a powder diffraction | |
650 | 4 | |a side-bounce monochromator | |
700 | 1 | |a Gomez, Ariel |e verfasserin |4 aut | |
700 | 1 | |a Diaz Moreno, Beatriz |e verfasserin |4 aut | |
700 | 1 | |a Muir, David |e verfasserin |4 aut | |
700 | 1 | |a Spasyuk, Denis |e verfasserin |4 aut | |
700 | 1 | |a King, Graham |e verfasserin |4 aut | |
700 | 1 | |a Reid, Joel W |e verfasserin |4 aut | |
700 | 1 | |a Kim, Chang Yong |e verfasserin |4 aut | |
700 | 1 | |a Kycia, Stefan |e verfasserin |4 aut | |
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