Facile Preparation of Activated Carbon from Peanut Shell for Determination of Bisphenol A in Human Urine by High-Performance Liquid Chromatography
Herein, a facile and low-cost method for the preparation of activated carbon from peanut shell was developed for the first time for the fast extraction and determination of Bisphenol A in human urine. Bisphenol A was separated by EC-C18 column (250 mm×4.6 mm, 4 μm) and was detected by VWD, with retention time for qualitative analysis and peak area for quantitation. The parameters, pH values of the urine, adsorbent dose, adsorption time and so on, were optimized to achieve the excellent extraction performance. The detection limit of Bisphenol A in human urine was 1.0 ng · mL-1 (S/N = 3), and the standard curve was linear in the range of 5.0 ng · mL-1˜200.0 ng · mL-1 (r = 0.9993). The average recovery of Bisphenol A was 78.5˜96.2% at three spiked levels in the range of 5.00 ng · mL-1˜200.00 ng·mL-1. The method was proved simple, practical and highly sensitive, which could satisfy the request for the determination of Bisphenol A in human urine.
| Medienart: |
E-Artikel |
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| Erscheinungsjahr: |
2021 |
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| Erschienen: |
2021 |
| Enthalten in: |
Zur Gesamtaufnahme - volume:21 |
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| Enthalten in: |
Journal of nanoscience and nanotechnology - 21(2021), 3 vom: 01. März, Seite 1439-1445 |
| Sprache: |
Englisch |
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| Beteiligte Personen: |
Shi, Yanpeng [VerfasserIn] |
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| Links: |
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| Themen: |
16291-96-6 |
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| Anmerkungen: |
Date Completed 11.06.2021 Date Revised 11.06.2021 published: Print Citation Status MEDLINE |
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| doi: |
10.1166/jnn.2021.18980 |
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| funding: |
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| Förderinstitution / Projekttitel: |
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| PPN (Katalog-ID): |
NLM319682021 |
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| 500 | |a Date Revised 11.06.2021 | ||
| 500 | |a published: Print | ||
| 500 | |a Citation Status MEDLINE | ||
| 520 | |a Herein, a facile and low-cost method for the preparation of activated carbon from peanut shell was developed for the first time for the fast extraction and determination of Bisphenol A in human urine. Bisphenol A was separated by EC-C18 column (250 mm×4.6 mm, 4 μm) and was detected by VWD, with retention time for qualitative analysis and peak area for quantitation. The parameters, pH values of the urine, adsorbent dose, adsorption time and so on, were optimized to achieve the excellent extraction performance. The detection limit of Bisphenol A in human urine was 1.0 ng · mL-1 (S/N = 3), and the standard curve was linear in the range of 5.0 ng · mL-1˜200.0 ng · mL-1 (r = 0.9993). The average recovery of Bisphenol A was 78.5˜96.2% at three spiked levels in the range of 5.00 ng · mL-1˜200.00 ng·mL-1. The method was proved simple, practical and highly sensitive, which could satisfy the request for the determination of Bisphenol A in human urine | ||
| 650 | 4 | |a Journal Article | |
| 650 | 4 | |a Research Support, Non-U.S. Gov't | |
| 650 | 7 | |a Benzhydryl Compounds |2 NLM | |
| 650 | 7 | |a Phenols |2 NLM | |
| 650 | 7 | |a Charcoal |2 NLM | |
| 650 | 7 | |a 16291-96-6 |2 NLM | |
| 650 | 7 | |a bisphenol A |2 NLM | |
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| 700 | 1 | |a Zhang, Lei |e verfasserin |4 aut | |
| 700 | 1 | |a Shao, Ji |e verfasserin |4 aut | |
| 700 | 1 | |a Shan, Xiaoyue |e verfasserin |4 aut | |
| 700 | 1 | |a Ye, Haipeng |e verfasserin |4 aut | |
| 700 | 1 | |a Tan, Siwei |e verfasserin |4 aut | |
| 700 | 1 | |a Chen, Jianrong |e verfasserin |4 aut | |
| 700 | 1 | |a Wu, Xilin |e verfasserin |4 aut | |
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