Does tin pre-treatment enhance the bond strength of adhesive systems to enamel?

Copyright © 2013 Elsevier Ltd. All rights reserved..

OBJECTIVES: The study investigated the modification of composite-to-enamel bond strength by pre-treatment of enamel with a concentrated, acidic SnCl2-solution.

METHODS: Six groups of flat human enamel specimens (n=44 per group) were treated as follows: OB-H: H3PO4 etching, Optibond FL application (primer+adhesive; manufacturer's instructions); OB-S: SnCl2 pre-treatment, Optibond FL application (primer+adhesive); OB-HS: H3PO4 etching+SnCl2 pre-treatment, Optibond FL application (primer+adhesive); CF-N: Clearfil SE application (primer+bond; manufacturer's instructions); CF-H: H3PO4 etching, Clearfil SE application (primer+bond); CF-S: SnCl2 pre-treatment, Clearfil SE application (primer+bond). Enamel specimens were then built up with resin composite (Clearfil Majesty Esthetic) and stored (100% humidity, 37 °C, 1 week). μTBS-measurement and failure mode analysis of one-half of the specimens were performed immediately after storage, while the other half was analysed after a thermocycling procedure (8500 cycles; 5 °C and 55 °C; dwell time 30s). Additional specimens were prepared for SEM- and EDX-analysis.

RESULTS: Highest values were measured for OB-H before and after thermocycling, lowest values for CF-N. Compared to OB-H treatment, OB-S treatment reduced μTBS before/after thermocycling by 23%/28% and OB-HS treatment by 8%/24% (except for OB-SH before (n.s.), all p≤0.001 compared to OB-H). In the Clearfil SE treated groups pre-treatment increased μTBS significantly compared to CF-N (before/after: CF-H: +46%/+70%; CF-S: +51%/42%; all p≤0.001).

CONCLUSION: Pre-treatment with H3PO4 or SnCl2 markedly increased the μTBS of Clearfil SE to enamel. However, thermocycling partly reduced the gain in μTBS obtained by SnCl2 pre-treatment.

CLINICAL SIGNIFICANCE: The application of an acidic and highly concentrated SnCl2 solution is a good option to increase the μTBS between enamel and a resin composite mediated by an adhesive system containing the multifunctional monomer MDP.

Medienart:

E-Artikel

Erscheinungsjahr:

2013

Erschienen:

2013

Enthalten in:

Zur Gesamtaufnahme - volume:41

Enthalten in:

Journal of dentistry - 41(2013), 7 vom: 01. Juli, Seite 642-52

Sprache:

Englisch

Beteiligte Personen:

Schlueter, Nadine [VerfasserIn]
Peutzfeldt, Anne [VerfasserIn]
Ganss, Carolina [VerfasserIn]
Lussi, Adrian [VerfasserIn]

Links:

Volltext

Themen:

1BQV3749L5
Clearfil SE Bond
Clearfil majesty
Comparative Study
Composite Resins
E4GA8884NN
Journal Article
OptiBond FL
Phosphoric Acids
Phosphoric acid
Resin Cements
Stannous chloride
Tin Compounds

Anmerkungen:

Date Completed 04.07.2014

Date Revised 24.06.2013

published: Print-Electronic

Citation Status MEDLINE

doi:

10.1016/j.jdent.2013.03.009

funding:

Förderinstitution / Projekttitel:

PPN (Katalog-ID):

NLM226604969