Synthesis of carbamates from diethoxycarbonyl hydrazine derivatives by E1cB eliminative cleavage of the N-N'-bond rather than reduction
Treatment of diethoxycarbonyl hydrazine derivatives with methyl bromoacetate/Cs(2)CO(3)/MeCN at 50 degrees C followed by heating to 80 degrees C resulted in N-N' bond cleavage to the corresponding carbamates.
| Medienart: |
E-Artikel |
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| Erscheinungsjahr: |
2009 |
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| Erschienen: |
2009 |
| Enthalten in: |
Zur Gesamtaufnahme - volume:11 |
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| Enthalten in: |
Organic letters - 11(2009), 24 vom: 17. Dez., Seite 5646-8 |
| Sprache: |
Englisch |
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| Beteiligte Personen: |
Magnus, Philip [VerfasserIn] |
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| Links: |
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| Themen: |
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| Anmerkungen: |
Date Completed 02.02.2010 Date Revised 16.12.2009 published: Print Citation Status PubMed-not-MEDLINE |
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| doi: |
10.1021/ol902313v |
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| funding: |
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| Förderinstitution / Projekttitel: |
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| PPN (Katalog-ID): |
NLM192788841 |
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| 520 | |a Treatment of diethoxycarbonyl hydrazine derivatives with methyl bromoacetate/Cs(2)CO(3)/MeCN at 50 degrees C followed by heating to 80 degrees C resulted in N-N' bond cleavage to the corresponding carbamates | ||
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| 700 | 1 | |a Seibert, Kimberly A |e verfasserin |4 aut | |
| 700 | 1 | |a Ornholt, Alexandra |e verfasserin |4 aut | |
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