Determination of 18 organophosphate pesticide residues in Flos Lonicerae
OBJECTIVE: To establish an analysical method for the quantitative determination of 18 kinds of organophosphate pesticide residues in Flos Lonicerae.
METHOD: The pesticides in samples were extracted with acetone by Ultrasonic wave Assistant Extraction (UAE), purified by Solid-Phase Extraction (SPE). Using PFPD detecter gas chromatography with HP-1701 column.
RESULT AND CONCLUSION: All 18 pesticides were separated well in 30 minutes. The detection limits was 4.0-18.0 microg x kg(-1). The range of recovery and RSD were 83.64%-88.65% and 2.8%-6.0%, respectively. And it met the requirements of pesticide multi-residues analysis.
| Medienart: |
Artikel |
|---|
| Erscheinungsjahr: |
2006 |
|---|---|
| Erschienen: |
2006 |
| Enthalten in: |
Zur Gesamtaufnahme - volume:31 |
|---|---|
| Enthalten in: |
Zhongguo Zhong yao za zhi = Zhongguo zhongyao zazhi = China journal of Chinese materia medica - 31(2006), 16 vom: 27. Aug., Seite 1321-3 |
| Sprache: |
Chinesisch |
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| Beteiligte Personen: |
Xiang, Zeng-Xu [VerfasserIn] |
|---|
| Themen: |
English Abstract |
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| Anmerkungen: |
Date Completed 20.11.2007 Date Revised 06.02.2008 published: Print Citation Status MEDLINE |
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| Förderinstitution / Projekttitel: |
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| PPN (Katalog-ID): |
NLM166179493 |
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| LEADER | 01000naa a22002652 4500 | ||
|---|---|---|---|
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| 041 | |a chi | ||
| 100 | 1 | |a Xiang, Zeng-Xu |e verfasserin |4 aut | |
| 245 | 1 | 0 | |a Determination of 18 organophosphate pesticide residues in Flos Lonicerae |
| 264 | 1 | |c 2006 | |
| 336 | |a Text |b txt |2 rdacontent | ||
| 337 | |a ohne Hilfsmittel zu benutzen |b n |2 rdamedia | ||
| 338 | |a Band |b nc |2 rdacarrier | ||
| 500 | |a Date Completed 20.11.2007 | ||
| 500 | |a Date Revised 06.02.2008 | ||
| 500 | |a published: Print | ||
| 500 | |a Citation Status MEDLINE | ||
| 520 | |a OBJECTIVE: To establish an analysical method for the quantitative determination of 18 kinds of organophosphate pesticide residues in Flos Lonicerae | ||
| 520 | |a METHOD: The pesticides in samples were extracted with acetone by Ultrasonic wave Assistant Extraction (UAE), purified by Solid-Phase Extraction (SPE). Using PFPD detecter gas chromatography with HP-1701 column | ||
| 520 | |a RESULT AND CONCLUSION: All 18 pesticides were separated well in 30 minutes. The detection limits was 4.0-18.0 microg x kg(-1). The range of recovery and RSD were 83.64%-88.65% and 2.8%-6.0%, respectively. And it met the requirements of pesticide multi-residues analysis | ||
| 650 | 4 | |a English Abstract | |
| 650 | 4 | |a Journal Article | |
| 650 | 7 | |a Organophosphorus Compounds |2 NLM | |
| 650 | 7 | |a Pesticide Residues |2 NLM | |
| 700 | 1 | |a Zhao, Wei-Jia |e verfasserin |4 aut | |
| 700 | 1 | |a Guo, Qiao-Sheng |e verfasserin |4 aut | |
| 773 | 0 | 8 | |i Enthalten in |t Zhongguo Zhong yao za zhi = Zhongguo zhongyao zazhi = China journal of Chinese materia medica |d 1989 |g 31(2006), 16 vom: 27. Aug., Seite 1321-3 |w (DE-627)NLM012733113 |x 1001-5302 |7 nnns |
| 773 | 1 | 8 | |g volume:31 |g year:2006 |g number:16 |g day:27 |g month:08 |g pages:1321-3 |
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| 952 | |d 31 |j 2006 |e 16 |b 27 |c 08 |h 1321-3 | ||