Comparing the mechanical properties, microstructure, texture and in-vitro degradation behavior of TNTZ/nano-fluorapatite composite and TNTZ bioalloy
Copyright © 2021 Elsevier Ltd. All rights reserved..
The present study deals with (i) the fabrication of the composite surface layer of Ti-29Nb-13Ta-4.6Zr/nano-fluorapatite through friction stir processing, (ii) clarifying the correlation of microstructure and texture with in-vitro degradation behavior and bioactivity of fabricated nano-biocomposite, and (iii) comparing the mechanical and functional properties of nano composite whit those obtained for TNTZ bio-alloy. The results indicated that increasing the number of deformation passes effectively refines the microstructure, leading to the average grain sizes of less than 5 μm. The texture of the material was also evolved in the presence of the nano particles where the grains reorient along <111> direction in contrast to the <101>-oriented grains in the starting microstructure. In-vitro bioactivity of the processed samples was measured after being immersed in simulated body fluid solution for various duration up to 30 days. Enhanced corrosion resistance and bio-mineralization of nanocomposite surface layer was discussed relying on the occurrence of grain refinement, substructure development and evolution of texture components along <101> direction. Assessment of the mechanical properties of the fabricated composites and as-received material also indicated the positive effect of the applied processing route and the presence of nano particles.
Medienart: |
E-Artikel |
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Erscheinungsjahr: |
2021 |
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Erschienen: |
2021 |
Enthalten in: |
Zur Gesamtaufnahme - volume:117 |
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Enthalten in: |
Journal of the mechanical behavior of biomedical materials - 117(2021) vom: 15. Mai, Seite 104402 |
Sprache: |
Englisch |
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Beteiligte Personen: |
Rajabi, F [VerfasserIn] |
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Links: |
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Themen: |
91D9GV0Z28 |
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Anmerkungen: |
Date Completed 14.05.2021 Date Revised 14.05.2021 published: Print-Electronic Citation Status MEDLINE |
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doi: |
10.1016/j.jmbbm.2021.104402 |
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funding: |
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Förderinstitution / Projekttitel: |
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PPN (Katalog-ID): |
NLM321802144 |
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500 | |a published: Print-Electronic | ||
500 | |a Citation Status MEDLINE | ||
520 | |a Copyright © 2021 Elsevier Ltd. All rights reserved. | ||
520 | |a The present study deals with (i) the fabrication of the composite surface layer of Ti-29Nb-13Ta-4.6Zr/nano-fluorapatite through friction stir processing, (ii) clarifying the correlation of microstructure and texture with in-vitro degradation behavior and bioactivity of fabricated nano-biocomposite, and (iii) comparing the mechanical and functional properties of nano composite whit those obtained for TNTZ bio-alloy. The results indicated that increasing the number of deformation passes effectively refines the microstructure, leading to the average grain sizes of less than 5 μm. The texture of the material was also evolved in the presence of the nano particles where the grains reorient along <111> direction in contrast to the <101>-oriented grains in the starting microstructure. In-vitro bioactivity of the processed samples was measured after being immersed in simulated body fluid solution for various duration up to 30 days. Enhanced corrosion resistance and bio-mineralization of nanocomposite surface layer was discussed relying on the occurrence of grain refinement, substructure development and evolution of texture components along <101> direction. Assessment of the mechanical properties of the fabricated composites and as-received material also indicated the positive effect of the applied processing route and the presence of nano particles | ||
650 | 4 | |a Journal Article | |
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