Comparing the mechanical properties, microstructure, texture and in-vitro degradation behavior of TNTZ/nano-fluorapatite composite and TNTZ bioalloy

Copyright © 2021 Elsevier Ltd. All rights reserved..

The present study deals with (i) the fabrication of the composite surface layer of Ti-29Nb-13Ta-4.6Zr/nano-fluorapatite through friction stir processing, (ii) clarifying the correlation of microstructure and texture with in-vitro degradation behavior and bioactivity of fabricated nano-biocomposite, and (iii) comparing the mechanical and functional properties of nano composite whit those obtained for TNTZ bio-alloy. The results indicated that increasing the number of deformation passes effectively refines the microstructure, leading to the average grain sizes of less than 5 μm. The texture of the material was also evolved in the presence of the nano particles where the grains reorient along <111> direction in contrast to the <101>-oriented grains in the starting microstructure. In-vitro bioactivity of the processed samples was measured after being immersed in simulated body fluid solution for various duration up to 30 days. Enhanced corrosion resistance and bio-mineralization of nanocomposite surface layer was discussed relying on the occurrence of grain refinement, substructure development and evolution of texture components along <101> direction. Assessment of the mechanical properties of the fabricated composites and as-received material also indicated the positive effect of the applied processing route and the presence of nano particles.

Medienart:

E-Artikel

Erscheinungsjahr:

2021

Erschienen:

2021

Enthalten in:

Zur Gesamtaufnahme - volume:117

Enthalten in:

Journal of the mechanical behavior of biomedical materials - 117(2021) vom: 15. Mai, Seite 104402

Sprache:

Englisch

Beteiligte Personen:

Rajabi, F [VerfasserIn]
Zarei-Hanzaki, A [VerfasserIn]
Abedi, H R [VerfasserIn]
Safdel, A [VerfasserIn]
Bertrand, E [VerfasserIn]

Links:

Volltext

Themen:

91D9GV0Z28
Biocompatibility
Corrosion resistance
Durapatite
Friction stir processing
Journal Article
Microstructure
Nanocomposite
Titanium alloy

Anmerkungen:

Date Completed 14.05.2021

Date Revised 14.05.2021

published: Print-Electronic

Citation Status MEDLINE

doi:

10.1016/j.jmbbm.2021.104402

funding:

Förderinstitution / Projekttitel:

PPN (Katalog-ID):

NLM321802144